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VERIFYING

VISCOSITY

V

iscosity is a physical property that

describes the resistance of fluid to

flow under stress. There are many

different types of viscosities,

e.g., dynamic, kinematic, intrinsic, and inherent,

amongst others. Dynamic and kinematic viscosities

are the most common across all industries. They both

relate to the resistance of a fluid to flow under stress.

However, for dynamic viscosity, the stress can be any

force applied to the fluid, whereas kinematic viscosity

focuses on gravity as the force applied on the fluid.

Practically speaking, kinematic viscosity can be

calculated using dynamic viscosity and density, as the ratio

of one to the other:

Where:

v

= kinematic viscosity (mm

2

/sec.).

η

= dynamic viscosity (mPa

.

sec.).

ρ

= density (g/cm

3

).

This article will explain how a technology used

to measure dynamic viscosity has been adapted

to measure kinematic viscosity. It will then

detail how this technology has been adapted

into an analyser to measure kinematic

viscosity at reference temperature. The

final section of this article will

present the results of the tests to

determine repeatability,

accuracy and

reproducibility of

the new viscosity at reference temperature

analyser.

Existing technology for

kinematic viscosity at reference

temperature

Viscosity measurement at reference temperature is a

measurement where the sample is drawn from the

process line at process temperature and brought to an

analyser with an internal temperature control system to

heat/cool the product to the desired temperature before

measuring the viscosity.

The main technique for this measurement uses the

Hallikainen

1

capillary measurement system combined

with an outside densitometer. Its drawbacks are the use

of an oil bath and its heavy maintenance requirements.

The technology used by capillary systems measures the

pressure difference between the inlet and the outlet of

the capillary to make a direct measurement of

viscosity. The capillary is inserted in an oil bath to

bring the sample to the required temperature and

ensure that the diameter and length of the

capillary do not change with temperature. Other

systems based on the same capillary technology

are available but use an oven instead of an oil

bath. This system is not compliant to the

reference method ASTM D445,

2

since it

uses a pump to flow the sample, it

measures the dynamic viscosity

and needs an external density

measurement and/or a

correlation.

Luc K. Bellière

and Philippe Burg, Sofraser,

France,

evaluate a new kinematic viscosity

analyser working at reference temperature.